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走进宝藏实验室——大连化物所

来源：布鲁克纳米分析部分类：成果 2024-03-28 14:15:09 8阅读次数

中国科学院大连化学物理研究所（简称“大连化物所”）是一个基础研究与应用研究并重、应用研究和技术转化相结合，以任务带学科为主要特色的综合性研究所，其重点学科领域为：催化化学、工程化学、化学激光和分子反应动力学以及近代分析化学和生物技术。

其中，能源研究技术平台是大连化物所公共技术中心，东北先进制造与材料的大型仪器区域中心的成员单位，中国科学院电镜技术联盟理事单位。旨在为全所各研究单元及社会提供分析测试服务和技术支撑，同时兼顾新方法和新技术的研发、高水平技术支撑人才的引进和培养。该平台配备了多台国际一流的先进科学仪器设备，充分提供测试服务、仪器设备运行维护、仪器功能和测试方法开及技术培训以满足所内科研工作需求。

近日，布鲁克应用进驻该平台进行仪器设备的应用专业化培训教学，先后对纳米分析表征仪器EDS/EBSD进行应用及技巧讲解，并携样品上机测试，解答使用平台人员的问题并进行操作指导，助力实验室研究人员在材料相关领域的分析研究工作，为广大科研工作者提供持续健康的技术和应用支持！

先进的化学成分和组织结构分析解决方案

适配于SEM和TEM的QUANTAX EDS

布鲁克第七代能谱仪QUANTAX XFlash^?7具有卓越的能量分辨率、输出计数率和最优的结构设计，可提供30 至 100 mm2多种有效晶体面积供选择。

QUANTAX WDS 平行光波谱仪

QUANTAX WDS XSense波谱仪集非磁性无畸变的平行光学设计和全新的的探测器技术于一身，紧凑的WDS系统能够在低能端进行超灵敏的高分辨率谱峰分析。

同轴TKD实现SEM最佳空间分辨率

纳米级金颗粒样品的原始取向图，放大区域为4~6nm的退火孪晶，图像比例尺为100nm。

SEM上的QUANTAX Micro-XRF

布鲁克第二代XTrace 2微区荧光光谱仪使用户以最小的成本，在SEM上使用微区XRF的全部功能。

SEM的微区XRF元素面扫描分析采自南非Newlands的伯利岩中含金刚石的地幔榴辉岩样品。主要相为石榴石和单斜辉石，含少量硫化物和交代矿物。分析面积约为3 cm x 2 cm.

原位定量纳米力学测试系统与TKD联用

纳米线和薄膜样品可以在独家的微电子“Push-to-Pull”压转拉装置上进行固定和测试。同轴TKD测试可以使用OPTIMUS 2探头完成，将TKD与PI 89相结合有助于理解样品在应变作用下的形变趋势。

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[8]未定义数组索引: page
[8]未定义数组下标: 0
[2]Declaration of app\common\model\News::getAllList($filter = Array, $limit = 16, $order = Array, $with = Array) should be compatible with app\common\model\BaseModel::getAllList($filter = Array, $with = Array, $limit = 0, $sort = Array, $field = 'a.*', $join = Array)
[2]Declaration of app\common\model\Company::getAllList($filter = Array, $limit = 20) should be compatible with app\common\model\BaseModel::getAllList($filter = Array, $with = Array, $limit = 0, $sort = Array, $field = 'a.*', $join = Array)
[8]未定义数组索引: center
[8]Only variables should be passed by reference
[2]Declaration of app\common\model\NewsComment::getAllList($filter = Array, $limit = 16) should be compatible with app\common\model\BaseModel::getAllList($filter = Array, $with = Array, $limit = 0, $sort = Array, $field = 'a.*', $join = Array)
[8192]Function create_function() is deprecated
[8192]Function create_function() is deprecated
[8]未定义数组索引: area
[8]未定义数组索引: st
[2]Declaration of app\common\model\Topic::getList($filter = Array) should be compatible with app\common\model\BaseModel::getList($filter = Array, $sort = Array)
[2]Declaration of app\common\model\Topic::getAllList($filter = Array, $field = 'id,md5,tit...', $limit = 0) should be compatible with app\common\model\BaseModel::getAllList($filter = Array, $with = Array, $limit = 0, $sort = Array, $field = 'a.*', $join = Array)
[2]Declaration of app\common\model\TopicInfoList::getAllList($filter = Array, $limit = 8) should be compatible with app\common\model\BaseModel::getAllList($filter = Array, $with = Array, $limit = 0, $sort = Array, $field = 'a.*', $join = Array)
[8]未定义数组索引: center
[8]未定义数组索引: cid
[8]未定义数组索引: cid
[8]未定义数组索引: cid
[8]未定义数组索引: cid
[8]未定义数组索引: cid
[8]未定义数组索引: cid
[8]未定义数组索引: cid
[8]未定义数组索引: cid
[8]未定义数组索引: cid
[8]未定义数组索引: cid
[8]未定义数组索引: goods_list
[8]未定义数组下标: 0
[8]未定义数组索引: center
[8]未定义数组索引: center
[8]未定义数组索引: center
[8]未定义数组索引: center
[2]Declaration of app\common\model\Tag::getAllList($filter = Array, $with = Array, $limit = 5) should be compatible with app\common\model\BaseModel::getAllList($filter = Array, $with = Array, $limit = 0, $sort = Array, $field = 'a.*', $join = Array)
[2]Declaration of app\common\model\Tag::remove($filter) should be compatible with app\common\model\BaseModel::remove($filter = Array)
[8]未定义数组索引: center
[8]未定义数组索引: wtt_list

[ DB ] CONNECT:[ UseTime:0.000345s ] mysql:host=127.0.0.1;port=3306;dbname=120med;charset=utf8
[ SQL ] SHOW COLUMNS FROM `news_category` [ RunTime:0.000931s ]
[ SQL ] SELECT `id`,`name` FROM `news_category` WHERE `is_show` = 1 [ RunTime:0.000260s ]
[ SQL ] SELECT * FROM `news_category` WHERE `parent_id` = 0 AND `is_show` = 1 ORDER BY `sort` ASC,`id` DESC [ RunTime:0.000202s ]
[ SQL ] SHOW COLUMNS FROM `company` [ RunTime:0.000925s ]
[ SQL ] SHOW COLUMNS FROM `news` [ RunTime:0.000706s ]
[ SQL ] SELECT * FROM `news` WHERE `md5` = '3481303b58b1e670' AND `review_status` = 1 LIMIT 1 [ RunTime:0.000264s ]
[ SQL ] SHOW COLUMNS FROM `user_info` [ RunTime:0.000740s ]
[ SQL ] SELECT * FROM `user_info` WHERE `user_id` = 789 [ RunTime:0.000662s ]
[ SQL ] SELECT * FROM `company` WHERE `id` = 907 [ RunTime:0.000186s ]
[ SQL ] SHOW COLUMNS FROM `news_text` [ RunTime:0.000697s ]
[ SQL ] SELECT * FROM `news_text` WHERE `news_id` = 6445 [ RunTime:0.025919s ]
[ SQL ] SHOW COLUMNS FROM `news_belong_category` [ RunTime:0.000892s ]
[ SQL ] SELECT * FROM `news_belong_category` WHERE `news_id` = 6445 [ RunTime:0.002871s ]
[ SQL ] SELECT * FROM `news_category` WHERE `id` IN (5) [ RunTime:0.000208s ]
[ SQL ] SHOW COLUMNS FROM `user_follow` [ RunTime:0.000850s ]
[ SQL ] SELECT `id` FROM `user_follow` WHERE `user_id` IS NULL AND `follow_user_id` = 789 LIMIT 1 [ RunTime:0.000377s ]
[ SQL ] SHOW COLUMNS FROM `news_comment` [ RunTime:0.000752s ]
[ SQL ] SELECT * FROM `news_comment` WHERE `news_id` = 6445 AND `parent_id` = 0 ORDER BY `id` DESC [ RunTime:0.000212s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `news_comment` WHERE `news_id` = 6445 LIMIT 1 [ RunTime:0.000208s ]
[ SQL ] SELECT * FROM `news` WHERE `is_show` = 1 AND `review_status` = 1 AND `id` IN (6445,584,7445,7413,7354,7129,7059,7010,7009,7008) ORDER BY field(id,6445,584,7445,7413,7354,7129,7059,7010,7009,7008) [ RunTime:0.000398s ]
[ SQL ] SELECT * FROM `user_info` WHERE `user_id` IN (789,156,696,247,714,577,294) [ RunTime:0.000693s ]
[ SQL ] SHOW COLUMNS FROM `topic` [ RunTime:0.000813s ]
[ SQL ] SELECT `id`,`md5`,`title`,`created_time` FROM `topic` WHERE `review_status` = 1 ORDER BY `id` DESC LIMIT 4 [ RunTime:0.000171s ]
[ SQL ] SHOW COLUMNS FROM `topic_info_list` [ RunTime:0.000699s ]
[ SQL ] SELECT * FROM `topic_info_list` WHERE `topic_id` = 1 ORDER BY `id` DESC LIMIT 2 [ RunTime:0.000185s ]
[ SQL ] SELECT * FROM `news` WHERE `id` IN (864,849) [ RunTime:0.000208s ]
[ SQL ] SELECT `id`,`md5`,`title`,`created_time` FROM `news` WHERE `review_status` = 1 AND `is_show` = 1 ORDER BY `id` DESC LIMIT 10 [ RunTime:0.000205s ]
[ SQL ] SHOW COLUMNS FROM `user` [ RunTime:0.000708s ]
[ SQL ] SELECT `a`.* FROM `user` `a` INNER JOIN `news` `b` ON `a`.`id`=`b`.`user_id` GROUP BY `a`.`id` ORDER BY `b`.`id` DESC LIMIT 10 [ RunTime:0.009052s ]
[ SQL ] SELECT * FROM `user_info` WHERE `user_id` IN (466,458,209,372,521,819,385,657,412,274) [ RunTime:0.000748s ]
[ SQL ] SHOW COLUMNS FROM `seo` [ RunTime:0.000914s ]
[ SQL ] SELECT * FROM `seo` WHERE `column_type` = '02' AND `page_type` = 'news' AND `info_id` = 6445 LIMIT 1 [ RunTime:0.000174s ]
[ SQL ] SELECT * FROM `news_belong_category` WHERE `news_id` = 6445 [ RunTime:0.002869s ]
[ SQL ] SELECT * FROM `news_belong_category` WHERE `news_id` = 584 [ RunTime:0.001579s ]
[ SQL ] SHOW COLUMNS FROM `tag` [ RunTime:0.000797s ]
[ SQL ] SELECT `md5` FROM `tag` WHERE `is_open` = 1 AND `tag` = '实验室' LIMIT 1 [ RunTime:0.000242s ]
[ SQL ] SELECT * FROM `news_belong_category` WHERE `news_id` = 7445 [ RunTime:0.002764s ]
[ SQL ] SELECT * FROM `news_belong_category` WHERE `news_id` = 7413 [ RunTime:0.001546s ]
[ SQL ] SELECT * FROM `news_belong_category` WHERE `news_id` = 7354 [ RunTime:0.001520s ]
[ SQL ] SELECT * FROM `news_belong_category` WHERE `news_id` = 7129 [ RunTime:0.001626s ]
[ SQL ] SELECT * FROM `news_belong_category` WHERE `news_id` = 7059 [ RunTime:0.001552s ]
[ SQL ] SELECT * FROM `news_belong_category` WHERE `news_id` = 7010 [ RunTime:0.001536s ]
[ SQL ] SELECT * FROM `news_belong_category` WHERE `news_id` = 7009 [ RunTime:0.001527s ]
[ SQL ] SELECT * FROM `news_belong_category` WHERE `news_id` = 7008 [ RunTime:0.001512s ]
[ SQL ] SELECT * FROM `user` WHERE `id` = 789 LIMIT 1 [ RunTime:0.000181s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `follow_user_id` = 466 LIMIT 1 [ RunTime:0.000174s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `user_id` = 466 LIMIT 1 [ RunTime:0.000136s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `follow_user_id` = 458 LIMIT 1 [ RunTime:0.000132s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `user_id` = 458 LIMIT 1 [ RunTime:0.000122s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `follow_user_id` = 209 LIMIT 1 [ RunTime:0.000136s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `user_id` = 209 LIMIT 1 [ RunTime:0.000126s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `follow_user_id` = 372 LIMIT 1 [ RunTime:0.000135s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `user_id` = 372 LIMIT 1 [ RunTime:0.000123s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `follow_user_id` = 521 LIMIT 1 [ RunTime:0.000127s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `user_id` = 521 LIMIT 1 [ RunTime:0.000122s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `follow_user_id` = 819 LIMIT 1 [ RunTime:0.000132s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `user_id` = 819 LIMIT 1 [ RunTime:0.000121s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `follow_user_id` = 385 LIMIT 1 [ RunTime:0.000129s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `user_id` = 385 LIMIT 1 [ RunTime:0.000133s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `follow_user_id` = 657 LIMIT 1 [ RunTime:0.000128s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `user_id` = 657 LIMIT 1 [ RunTime:0.000124s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `follow_user_id` = 412 LIMIT 1 [ RunTime:0.000122s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `user_id` = 412 LIMIT 1 [ RunTime:0.000136s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `follow_user_id` = 274 LIMIT 1 [ RunTime:0.000192s ]
[ SQL ] SELECT COUNT(*) AS tp_count FROM `user_follow` WHERE `user_id` = 274 LIMIT 1 [ RunTime:0.000171s ]

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